News | Rex Heat Treat

Controlled Atmosphere Heat Treating for AMS-Spec Compliance

Written by Miles IT | Feb 2, 2026 2:48:18 PM

Key Takeaways:

  • Defense industry components must meet strict military specifications (AMS and MIL-Spec) requiring absolute reliability, repeatable performance, and full traceability.

  • Traditional open-air furnaces are unsuitable for critical defense alloy steel parts with finished or near-net-machined surfaces because atmospheric oxygen causes oxidation (scale) and decarburization (decarb), inevitably leading to part failure.

  • Controlled atmosphere heat treating is the only way to guarantee 100% Specification compliance.

  • Rex Heat Treat offers the level of compliance required to meet AMS and MIL-Spec heat treat standards.

In the defense and aerospace industries, there are no margins for error. Whether on land, at sea, or in the air, the reliability of a single component can be the difference between mission success and catastrophic failure. 

This zero-failure tolerance isn't just a goal; it's a hard-line requirement built into every contract. This directive flows down to every part, governed by rigid military and aerospace specifications that dictate exact material properties, from surface hardness to core mechanical strength.

For critical components—especially those forged from advanced alloy steel—achieving these precise mechanical properties is often impossible with conventional, open-air heat treating. This is where controlled atmosphere heat treating becomes the non-negotiable solution, providing the only path to guarantee 100% heat treat compliance.

What Heat Treat Specifications Demand from Metal Components

When a component is “Spec compliant," it means it meets the rigid standards set by the U.S. Department of Defense, such as MIL-STD or Aerospace Material Specifications (AMS) like AMS 2759. This isn't just a quality suggestion; it's a guarantee that the part will perform its exact function reliably under extreme, life-or-death conditions. For defense contractors, these standards are the foundation of their heat treatment supply chain.

Unlike in commercial applications, "close enough" is not an option. AMS and MIL specifications demand verifiable proof that a part meets three core requirements:

  • Absolute Reliability & Repeatability: The first part must be 100% identical in its mechanical properties to the ten-thousandth part. The heat treat process must be so tightly controlled that the outcome is a guaranteed constant.

  • Extreme Performance: These components must deliver unmatched fatigue strength, high wear resistance, and corrosion resistance to withstand battlefield (or in-flight) conditions. This performance is achieved through the heat-treating process, and it must be perfect.

  • Complete Traceability: Every step, from the raw material to the final heat treat cycle, must be documented. A full, unbroken data chain—including furnace charts and certifications—is required to prove, without a doubt, that the component is compliant. This may also mean serial number traceability is maintained. Heat Codes are also extremely critical when heat treating for the Aerospace and Defense industries—even a 0.01% difference between multiple material heat lot compositions can completely change the heat treat atmosphere requirement, like the Carbon content control. 

This is the unforgiving landscape where defense and aerospace suppliers operate. They cannot risk a contract or, more importantly, a mission on a heat treater who can't prove their process.

What Happens in an Uncontrolled Atmosphere

In traditional furnaces, the open air quality introduces oxygen and other gases to the heat treatment process, which can be disastrous for alloys needing to meet specification compliance standards. That’s because heating a high-strength alloy steel part to 1500°F is a violent, reactive process, making it that much more imperative that spec compliance be considered every step of the way.

This uncontrolled atmosphere creates two challenges that are catastrophic for steel processing for defense applications:

Oxidation (Scale):

This is the most obvious problem. The oxygen in the air reacts with the hot metal, forming a brittle, flaky layer of oxide, or "scale." This scale destroys precise surface finishes, can clog critical threads on fasteners, and interferes with subsequent coatings. Removing it requires costly and damaging post-processing like machining, chem milling, and sandblasting, which can itself violate a material's requirements by altering dimensions or component integrity.

Decarburization ("Decarb"):

This is the more insidious, invisible threat. Carbon is a critical element that gives alloy steel its hardness and strength. In an uncontrolled atmosphere, the Carbon atoms on the surface of the part are drawn out and burned off. This creates a soft, weak "skin" on a component that was specifically designed to be hard. A part with decarb will fail fatigue testing every time, guaranteeing a field failure.

For defense and aerospace applications, both oxidation and decarb are grounds for immediate rejection. A component that is soft on the surface or has scale buildup is, by definition, a non-compliant part.

How Controlled Atmosphere Heat Treating Works

Controlled Atmosphere Heat Treating is the definitive solution to the problems of oxidation and decarb. This process involves heating and cooling components inside a sealed furnace where the gaseous environment is precisely formulated, monitored, and maintained throughout the entire cycle.

This controlled atmosphere isn't just air; it's a specific, engineered gas mixture. It can be:

Inert (Protective):

Using gases like pure Nitrogen or Argon, we create a protective "bubble" around the parts. This environment is non-reactive, preventing any chemical change from occurring. This is ideal for ensuring critical parts come out perfectly bright and clean with no scale.

Active (Reactive):

This is where the true precision of steel processing for defense applications comes in. We use specific gas mixtures (like endothermic gas) that are precisely balanced to interact with the steel in a predictable, desirable way.

What distinguishes a NADCAP heat treat expert from a standard facility is the control system. Advanced sensors, such as Carbonprobes, are used to continuously monitor the atmosphere's Carbon potential. This rigorous monitoring enables us to precisely align the Carbon content of the atmosphere with that of the alloy steel undergoing treatment.

This total control means your heat treat partner can guarantee zero decarb and zero unintended carburization. Furthermore, the entire process—from gas flow to temperature and time—is automated and computer-controlled, ensuring the process is 100% documented and, most importantly, 100% repeatable.

Active Atmospheres for Advanced Steel Processing

A controlled atmosphere isn't just a protective shield; it's a precision manufacturing tool. For advanced steel processing for defense applications, active atmospheres are used to deliberately change the chemistry of a component's surface, building parts that are stronger, tougher, and more durable than the raw alloy steel alone.

This is where true mastery of the mil-spec heat treat process comes into play.

Case Hardening (Carburizing):

Many military and aerospace components, like gears or shafts, need a dual property: an incredibly hard, wear-resistant surface with a softer, ductile core that can absorb shock and impact. We achieve this by running the parts in a sealed, Carbon-rich atmosphere. The Carbon actively concentrates into the surface of the steel, creating a deep, hardened "case" while the core remains tough.

The Rex Heat Treat Guarantee

The most advanced furnace in the world is useless if the team running it doesn't understand the mission. A compliant heat treated component requires a system of total quality, which is the core of the Rex Heat Treat difference.

Other ways we stand out:

  • Rex Heat Treat ensures Specification compliance with critical accreditations like NADCAP and ISO 9001:2015, proving our audited processes meet demanding defense and aerospace standards.

  • OEM/Prime Approved Suppliers Lists—Rex Heat Treat has achieved the trust of many end-users, like L3Harris, General Dynamics, Rocketdyne, Northrop, Lockheed Martin, Sikorsky, Boeing, Bell Helicopter, and more.

  • Our on-staff metallurgists optimize heat treatment for your specific alloy, ensuring maximum performance and 100% compliance.

  • Every cycle is digitally monitored and recorded, providing the complete data package (furnace charts, logs, and certification) for the verifiable traceability required by the DOD, giving your team peace of mind.

If you need the best in Aerospace and Military heat treat compliance, look no further than the experts at Rex Heat Treat. You can contact us today to find a solution for tomorrow.